Synthesis of a Thiol Building Block for the Crystallization of a Semiconducting Gyroidal Metal-sulfur Framework
by
 
He, Yonghe

Title
: 
Synthesis of a Thiol Building Block for the Crystallization of a Semiconducting Gyroidal Metal-sulfur Framework

Author
: 
He, Yonghe

Personal Author
: 
He, Yonghe

Publication Information
: 
Cambridge, MA MyJoVE Corp 2016

Physical Description
: 
online resource (750 seconds)

Series
: 
Chemistry

General Note
: 
Title from resource description page

Abstract
: 
Here, we present a one-pot, transition-metal-free synthesis of thiols and thioesters from aromatic halides and sodium thiomethoxide, followed by the preparation of single crystals of a metal-dithiolene network using thiol species generated in situ from the more stable and tractable thioester.

Reading Level
: 
For undergraduate, graduate, and professional students

Subject Term
: 
Chemistry

Electronic Access
: 
https://www.jove.com/t/57455


LibraryMaterial TypeItem BarcodeShelf NumberStatus
IYTE LibraryOnline Video2251458-1001XX(2251458.1)JoVe Video Online