Accessing Valuable Ligand Supports for Transition Metals: A Modified, Intermediate Scale Preparation of 1,2,3,4,5-Pentamethylcyclopentadiene
by
Call, Zachary
Title
:
Accessing Valuable Ligand Supports for Transition Metals: A Modified, Intermediate Scale Preparation of 1,2,3,4,5-Pentamethylcyclopentadiene
Author
:
Call, Zachary
Personal Author
:
Call, Zachary
Publication Information
:
Cambridge, MA MyJoVE Corp 2016
Physical Description
:
online resource (585 seconds)
Series
:
Chemistry
General Note
:
Title from resource description page
Abstract
:
Reliable, intermediate scale preparation of 1,2,3,4,5-pentamethylcyclopentadiene (Cp*H) is presented. The revised protocol for the synthesis and purification of the ligand minimizes the need for specialized laboratory equipment while simplifying reaction workups and product purification. Use of Cp*H in the synthesis of [Cp*MCl2]2 complexes (M = Ru, Ir) is also described.
Reading Level
:
For undergraduate, graduate, and professional students
Subject Term
:
Chemistry
Electronic Access
:
| Library | Material Type | Item Barcode | Shelf Number | Status |
|---|
| IYTE Library | Online Video | 2252776-1001 | XX(2252776.1) | JoVe Video Online |