Cover image for Chapters in the Evolution of Chromatography.
Chapters in the Evolution of Chromatography.
Title:
Chapters in the Evolution of Chromatography.
Author:
Ettre, Leslie S.
ISBN:
9781860949449
Personal Author:
Physical Description:
1 online resource (492 pages)
Contents:
Contents -- Preface -- Acknowledgments -- Introduction: One Hundred Years of Chromatography -- Steps in the Evolution of Chromatography -- References -- Part One: THE PRECURSORS OF CHROMATOGRAPHY -- 1. Chromatography in the Ancient World -- 1.1. Was Moses The First Chromatographer? -- 1.2. Did Pliny The Elder Use Planar Chromatography? -- References -- 2. Friedlieb Ferdinand Runge: "Self-Grown Pictures" as Precursors of Paper Chromatography -- 2.1. Runge's Life and Activities -- 2.2. Runge's Chemistry Textbooks -- 2.3. Investigation of Dyes -- 2.4. The Formation of Characteristic Patterns -- 2.5. Runge's Philosophy Concerning The "Self-Grown Pictures" -- 2.6. The "Od" -- 2.7. Runge's "Self-Grown Pictures" and Chromatography -- References -- 3. Early Petroleum Chromatographers -- 3.1. David T. Day -- 3.2. Joseph E. Gilpin -- 3.3. Carl Engler -- 3.4. Other Scientists -- 3.4.1. Leo Ubbelohde -- 3.4.2. Russian Petroleum Chemists -- 3.5. Controversy -- 3.6. Chromatography and the Cold War -- References -- Part Two: M. S. TSWETT AND THE DISCOVERY OF CHROMATOGRAPHY -- 4. M. S. Tswett, and the Invention of Chromatography Part I: Life and Early Work (1872-1903) -- 4.1. The Life of M. S. Tswett -- 4.2. Early Investigations -- 4.3. In Warsaw (1901-1903) -- References -- 5. M. S. Tswett and the Invention of Chromatography Part II: Completion of the Development (1903-1910) -- 5.1. Controversy -- 5.2. Tswett's Two Publications On Chromatography -- 5.3. Polemics -- 5.4. Tswett's 1910 Book -- 5.5. Postwords -- References -- 6. M. S. Tswett and the 1918 Nobel Prize in Chemistry -- 6.1. The Nobel Prizes -- 6.2. The Nominations for the 1918 Chemistry Prize -- 6.3. Tswett's Nomination -- 6.4. Evaluation -- References -- Part Three: THE FIRST PIONEERS IN THE USE OF CHROMATOGRAPHY -- 7. Gottfried Kränzlin, the First Follower of Tswett -- 7.1. G. Kränzlin and his Work.

7.2. Kränzlin's Thesis -- 7.3. Chromatography in Kränzlin's Thesis -- 7.4. Kränzlin's Place in the Evolution of Chromatography -- 7.5. Postscript -- References -- 8. Charles Dhéré - Pioneer and Tswett Biographer -- 8.1. Dhéré's Life -- His Field of Interest -- 8.2. Rogowski and His Chromatography Work -- 8.2.1. Rogowski's Life -- 8.2.2. Rogowski's Thesis Work -- 8.2.3. Dhéré and Tswett -- 8.3. Vegezzi and His Thesis Work -- 8.4. Later Work of Dhéré -- 8.5. Dhéré's Paper on Tswett -- 8.6. Conclusions -- References -- 9. L. S. Palmer and the Beginnings of Chromatography in the United States -- 9.1. Palmer's Life -- 9.2. Palmer's Research Activities -- 9.3. Chromatography in Palmer's Work -- 9.4. Chromatography in Palmer's Book -- 9.5. Palmer as the Transition Between Tswett and The "Rebirth" of Chromatography -- References -- 10. Katharine Hope Coward: A Pioneering User of Chromatography -- 10.1. K. H. Coward - Her Life -- 10.2. The State of Science in Coward's Time -- 10.2.1. Nutrition and Vitamins -- 10.2.2. Carotenoids -- 10.3. The Scope of Coward's Work in the 1920s -- 10.3.1. Coward and Chromatography -- 10.4. Postscript -- References -- 11. Theodor Lippmaa, A Forgotten Chromatographer -- 11.1. The Separation of Carotenoids -- 11.2. Postscript -- References -- Part Four: THE REBIRTH OF CHROMATOGRAPHY -- 12. The Rebirth of Chromatography -- 12.1. Richard Kuhn -- 12.2. The Field of Carotenoids -- 12.3. Edgar Lederer and the Rebirth of Chromatography -- 12.4. Further Activities -- References -- 13. The Rapid Spreading of the Technique -- 13.1. The Zurich Schools -- 13.2. Activities of Zechmeister -- 13.3. Beginnings of Inorganic Chromatography -- 13.4. Flow-Through Chromatograms -- References -- Part Five: THE EVOLUTION OF THE CHROMATOGRAPHIC TECHNIQUES -- 14. The Development of Partition Chromatography -- 14.1. The Start at Cambridge University.

14.2. The Birth of Partition Chromatography -- 14.3. Gas-Liquid Partition Chromatography -- References -- 15. Paper Chromatography -- 15.1. The Precursors -- 15.1.1. F. F. Runge -- 15.1.2. Capillary Analysis -- 15.2. The Invention of Paper Chromatography -- References -- 16. The Evolution of Thin-Layer Chromatography -- 16.1. The Beginnings -- 16.2. TLC Matures -- 16.3. The Activities of Egon Stahl -- 16.4. High Performance TLC -- 16.5. Forced-Flow TLC -- 16.6. Newer Developments -- References -- Part Six: ION-EXCHANGE CHROMATOGRAPHY -- 17. Preparative Ion-Exchange Chromatography and the Manhattan Project -- 17.1. Background -- 17.2. The Rare Earth Project at Ames -- 17.2.1. Methodology -- 17.2.2. Separation of the Individual Rare Earths -- 17.2.3. Displacement Ion-Exchange Chromatography -- 17.3. Postscript -- References -- 18. The Development of the Amino Acid Analyzer -- 18.1. Amino Acid Research at the Rockefeller Institute -- 18.2. Production of the Amino Acid Analyzer -- 18.3. Other Methods -- References -- Part Seven: GAS CHROMATOGRAPHY -- 19. Early Development of Gas Adsorption Chromatography -- 19.1. Analysis of Natural Gas -- 19.2. Claesson's System -- 19.3. Gerhard Hesse -- 19.4. The First Real Gas Chromatograph of Cremer -- 19.5. C. S. G. Phillips -- References -- 20. The Janák-Type Gas Chromatographs of the 1950s -- References -- 21. The Beginning of GC Instrumentation -- 21.1. Burrell's Kromo-Tog -- 21.2. Perkin-Elmer's Vapor Fractometer -- 21.3. Additional Instruments -- References -- 22. The Invention, Development, and Triumph of the Flame-Ionization Detector -- 22.1. Background -- 22.2. Invention -- 22.2.1. Work in Australia -- 22.2.2. Work in South Africa -- 22.3. Further Developments -- 22.4. Instrumentation -- 22.5. Patents -- 22.6. Triumph -- 22.7. Personalities -- References.

23. The Development of the Electron-Capture Detector -- 23.1. Inventions -- 23.1.1. First Stage: An Anemometer -- 23.1.2. Second Stage: Search for a High-Sensitivity Detector -- 23.1.3. Third State: The AID -- 23.1.4. Fourth State: The Invention of the ECD -- 23.2. Commercial Realization of the ECD -- 23.3. The Electron Capture Detector and the Environmental Movement -- 23.3.1. The Chlorofluorocarbon Problem -- References -- 24. Evolution of Open-Tubular (Capillary) Columns for Gas Chromatography -- 24.1. Invention -- 24.2. Realization -- 24.3. Columns Made of Metal -- 24.4. Coating Technique -- 24.5. Columns Made of Plastic Tubing -- 24.6. The Era of Glass Capillary Columns -- 24.7. Fused-Silica Columns -- 24.8. Immobilized and Bonded Stationary Phases -- References -- 25. The Beginnings of Headspace Analysis -- 25.1. First Uses of Headspace Sampling -- 25.2. Investigation of Food Volatiles -- 25.3. Determination of Alcohol in Blood -- 25.4. Automated and Integrated HSGC Systems -- References -- Part Eight: MODERN LIQUID CHROMATOGRAPHY -- 26. The Evolution of Modern Liquid Chromatography -- 26.1. From LC to HPLC -- 26.2. The Basics of HPLC -- 26.2.1. Name -- 26.2.2. Differences -- 26.3. Pioneers in HPLC -- 26.4. Bonded Phases -- References -- 27. The Development of the First High-Pressure Liquid Chromatograph at Yale University -- 27.1. Personalities -- 27.2. The Development of the First High-Pressure Liquid Chromatograph -- 27.3. The Rapid Spreading of HPLC -- 27.4. Nomenclature -- 27.5. Postscript -- References -- 28. The Development of GPC and the First Commercial HPLC Instruments -- 28.1. Early Activities -- 28.2. The Breakthrough: GPC -- 28.3. Liquid Chromatography -- References -- Part Nine: THE MOST IMPORTANT CHROMATOGRAPHY MEETINGS -- 29. Two Early Chromatography Symposia -- 29.1. The 1946 Conference on Chromatography.

29.2. The 1949 Faraday Society Symposium -- 29.2.1. Theory -- 29.2.2. Partition Chromatography -- 29.2.3. Adsorbents -- 29.2.4. Ion-Exchange Chromatography -- 29.2.5. Separation by Molecular Size -- 29.2.6. Gas Chromatography -- References -- 30. Early European Symposia Showing the Direction for the Evolution of Gas Chromatography -- 30.1. The Start of GC in England -- 30.2. The Ardeer Symposium -- 30.3. The 1956 London Symposium -- 30.4. The 1958 Amsterdam Symposium -- References -- 31. Early GC Symposia in the United States -- 31.1. The Early American Symposia -- 31.2. The 1956 Dallas ACS Symposium -- 31.3. The 1957 ISA Symposium -- 31.4. The 1959 ISA Symposium -- 31.5. The 1958 Conference of the New York Academy of Sciences -- References -- 32. Two Symposia, When HPLC was Young -- 32.1. The 1969 Las Vegas Symposium -- 32.2. The 1973 Interlaken Symposium -- References -- Index.
Abstract:
Chromatography, invented more than 100 years ago, is the most widely used separation technique in the world today. It has helped the birth of modern analytical instrumentation and continues to strongly influence the profiles of our chemical, biochemical and clinical laboratories.This book deals with the history of the invention and evolution of chromatography and of the various chromatographic techniques. After discussing the precursors, it elaborates on the activities of M.S. Tswett, the inventor of the technique, and of a few selected key pioneers. It then summarizes the evolution of the various branches of chromatography (planar, ion-exchange, gas and liquid), and also reviews the key role of international symposia in setting the trends in this evolution. Except for individual publications of the author, the history of the evolution of chromatography has not been the subject of any book. Thus, this book fills a major gap in the scientific literature.
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Electronic reproduction. Ann Arbor, Michigan : ProQuest Ebook Central, 2017. Available via World Wide Web. Access may be limited to ProQuest Ebook Central affiliated libraries.
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