Front Cover -- Modern Inorganic Synthetic Chemistry -- Copyright -- Contents -- Foreword -- Preface -- Contributors -- Chapter 1 Introduction - Frontiers in Modern Inorganic Synthetic Chemistry -- 1.1 Development Of New Synthetic Reactions, Synthetic Routes, Technologies And Associated Basic Scientific Studies -- 1.2 Basic Research in Support of Green Synthesis -- 1.3 Basic Research on Synthetic and Preparative Routes Under Extreme Conditions -- 1.4 Biomimetic Synthesis and Applications of Biotechnology in Inorganic Synthesis -- 1.5 Rational Synthesis and Molecular Engineering of Inorganic Compounds with Specific Structures and Functions -- References -- Chapter 2 High-temperature Synthesis -- 2.1 Attainment of high temperature-laboratory furnaces [1] and related techniques [2-6] -- 2.2 Types of high-temperature synthetic reactions and routes -- 2.3 High-temperature solid-state reaction [11-14] -- 2.4 Preparation Of Rare Earthcontaining Materials -- 2.5 Sol-gel process and precursors in high-temperature solid synthesis [45-47] -- 2.6 Self-Propagating Hightemperature Synthesis (Shs) [51- 60] -- 2.7 High-Temperature Preparation Of Metal Vapors And Active Molecules For Use In Cryosynthesis [70-72] -- 2.8 High-temperature electrolysis in molten salt system [73-79] -- References -- Chapter 3 Synthesis and Purification at Low Temperature -- 3.1 Attainment And Measurement Of Low And Ultralow Temperatures -- 3.2 Vacuum Technique and its Application in Inorganic Synthesis -- 3.3 Purification and Separation of Inorganics at Low Temperature -- 3.4 The Synthesis of Volatile Inorganic Compounds at Low Temperature -- 3.5 Formation of Rare-gas Molecules at Cryogenic Condition -- 3.6 Inorganic Synthesis in Liquid Ammonia -- 3.7 Cryosynthesis of Unusual Inorganic Compounds [52-55] -- References -- Chapter 4 Hydrothermal and Solvothermal Syntheses.

4.1 Foundation of Hydrothermal and Solvothermal Syntheses [1] -- 4.2 Functional Materials from Hydrothermal and Solvothermal Systems -- 4.3 Hydrothermal Biochemistry -- 4.4 Supercritical Water-a Novel Reaction System [106-110] -- 4.5 Techniques and Methods -- 4.6 Ionothermal Synthesis -- References -- Chapter 5 High Pressure Synthesis and Preparation of Inorganic Materials -- 5.1 Experimental Methods Of Inorganic Synthesis Under High Pressure -- 5.2 Effects Of High Pressure On Basic States Of Matters -- 5.3 Effects Of High Pressure On Inorganic Chemical Reactions -- 5.4 Effects Of High Pressure On Crystal And Electronic Structures Of Inorganic Compounds -- 5.5 Major Roles Of High Pressure Method In Inorganic Synthesis -- 5.6 Some Important Inorganic Compounds Synthesized Under High Pressure -- References -- Chapter 6 Inorganic Photochemical Synthesis -- 6.1 The Basic Concepts -- 6.2 Experimental Techniques -- 6.3 Photochemical Synthesis Of Organometallic Complexes -- 6.4 Photochemical Synthesis Of Inorganic Compounds -- 6.5 Synthesis Of Inorganic Thin Films Via Photochemical Reactions -- 6.6 Photochemical Synthesis of Nanomaterials -- 6.7 Production of H2 Via Photodecomposition of Water -- 6.8 Summary -- References -- Chapter 7 CVD and its Related Theories in Inorganic Synthesis and Materials Preparations -- 7.1 Brief History of Chemical Vapor Deposition -- 7.2 Technical Fundamentals of CVD -- 7.3 Equipment of Chemical Vapor Deposition -- 7.4 Some Theoretical Models of CVD Technology -- 7.5 Thermodynamic Coupling During The Low-Pressure Cvd Diamond Growth -- 7.6 Nonequilibrium Phase Diagrams For The Low-Pressure Cvd Diamond Growth -- References -- Chapter 8 Microwave-assisted Inorganic Syntheses -- 8.1 Basic Principle Of Microwave Radiation, Microwave Heating, And Microwave Equipment -- 8.2 Synthesis Of Inorganic Materials Under Microwave Heating.

8.3 Synthesis Of Inorganic Materials Assisted With Different Microwave Frequencies -- 8.4 Plasma-Assisted Synthesis Of Inorganic Materials -- 8.5 Some Of The Basic Conclusions And Outlooks About Microwave Radiation Associated Chemistry -- References -- Chapter 9 Syntheses of Coordination Compounds -- 9.1 Direct Synthesis Method -- 9.2 Component Exchange Method [2,3,15] -- 9.3 Redox Interaction Method [3] -- 9.5 Inclusion Complexation Method -- References -- Chapter 10 Assembly Chemistry of Coordination Polymers -- 10.1 Molecular Design Of Coordination Polymers -- 10.2 Structural Modulation By Reaction Conditions -- 10.3 Situ Metal/Ligand Reactions -- References -- Chapter 11 Synthetic Chemistry of Cluster Compounds -- 11.1 Description of the Clusters -- 11.2 Synthesis Of The Oxo Tm Clusters Under Hydrothermal Conditions -- 11.2.4 Designed Synthesis Via The Peripheral Substitution Of Ni6pw9 Sbus -- 11.3 Synthesis Of The Oxo Lanthanide Clusters Under Hydrothermal Conditions -- 11.3.1 Induced Synthesis Via The Ligands -- 11.4 Synthesis Of The Oxo Main Group Clusters Under Hydrothermal Conditions -- 11.5 Synthesis Of The Chalcogenide Clusters Under Hydro(Solvo)Thermal Conditions -- References -- Chapter 12 Synthetic Chemistry of Fullerenes -- 12.1 Synthesis -- 12.2 Characterization of Fullerenes -- 12.3 Chemical Reactions -- References -- Chapter 13 Synthesis of Organometallic Organometallic Compounds -- 13.1 Synthetic Reactions -- 13.2 Preparation of Typical Organometallic Compounds -- 13.3 Experimental Techniques -- References -- Chapter 14 Synthesis and Assembly Chemistry of Inorganic Polymers -- 14.1 Polyphosphazenes -- 14.2 Synthesis and Assembly Chemistry of Cyclophosphazene -- 14.3 Applications of Cyclomatrix Polyphosphazenes -- 14.4 Silicones -- References -- Chapter 15 Synthetic Chemistry of Nonstoichiometric Compounds.

15.1 Nonstoichiometric Compounds -- 15.2 Preparation of Nonstoichiometric Compounds -- 15.3 Characterization Of Nonstoichiometric Compounds -- References -- Chapter 16 Synthetic Chemistry of the Inorganic Ordered Porous Materials -- 16.1 Porous Materials -- 16.2 Zeolite and its Structure -- 16.3 The Synthesis of Zeolite -- 16.4 Zeotype: Zeolite-like Materials -- 16.5 New Strategies and New Trends of Zeolite Synthesis -- 16.6 Basic of Ordered Mesoporous Materials -- 16.7 Understanding the Synthesis of Mesoporous Materials -- 16.8 Typical Mesostructures and Mesoporous Materials -- 16.9 Synthesis Strategies for Mesoporous Silica -- 16.10 Morphology Control in Mesoporous Materials -- 16.11 New Compositions: Nonsilica-based Mesoporous Materials [13,22] -- 16.12 Porous Carbon Materials -- 16.13 Ordered Macroporous Materials -- 16.14 Challenges for Porous Material Scientist -- References -- Chapter 17 Assembly Chemistry of Anion-intercalated Layered Materials -- 17.1 Structure of Anion-intercalated Layered Materials -- 17.2 Preparative Chemistry of Anion-intercalated Layered Materials -- 17.3 Assembly Chemistry of Anion-intercalated Layered Materials -- References -- Chapter 18 Host-guest Functional Materials -- 18.1 Metal Clusters in Zeolites -- 18.2 Encapsulation of Dyes in Zeolites -- 18.3 Polymers and Carbon Matters in Zeolites -- 18.4 Semiconductor Nanoparticles in Zeolites -- 18.5 Metal Complexes in Molecular Sieves -- References -- Chapter 19 Chemical Preparation of Advanced Ceramic Materials -- 19.1 Nanoceramics -- 19.2Ceramic Matrix Composites (CMCs) -- 19.3 Integration Of Structures And Functions -- 19.4 Transparent Ceramics -- References -- Chapter 20 Amorphous Materials -- 20.1 Amorphous Structure -- 20.2 Formation Rule of Amorphous Alloy -- 20.3 Preparation Technology of Amorphous Materials -- 20.4 Bulk Amorphous Alloy-based Composite Materials.

References -- Chapter 21 Synthetic Chemistry of Nanomaterials -- 21.1 Basics of the Synthetic Chemistry of Nanomaterials -- 21.2 Synthetic Method for Nanomaterials -- 21.3 Synthesis of Nanomaterials -- 21.4 Concluding Remarks -- References -- Chapter 22 Preparation Chemistry of Inorganic Membranes -- 22.1 Inorganic MembranesInorganic Membranes and Their Major Characteristics -- 22.2 Synthesis of Microporous Inorganic Membranes -- 22.3 Synthesis of Ordered Mesoporous Membranes -- 22.4 Conclusions -- References -- Chapter 23 The Frontier of Inorganic Synthesis and Preparative Chemistry (I)-Biomimetic Synthesis -- 23.1 Biomineralization and Its Mimetic Inorganic Materials -- 23.2 Biotemplated Inorganic Materials -- 23.3 Biomimetic Synthesis of Inorganic Chiral Materials -- 23.4 Bio-inspired Multiscale Inorganic Materials -- References -- Chapter 24 Frontier of Inorganic Synthesis and Preparative Chemistry (II)-Designed SynthesisdInorganic Crystalline Porous Materials -- 24.1 Structure Design of Inorganic Crystalline Porous Materials -- 24.2 Chemical and Physical Problems on Way to the Rational Synthesis of Inorganic Crystalline Porous Materials -- 24.3 Attempts to the Rational Synthesis of Inorganic Porous Crystalline Materials -- 24.4 Future Perspective On The Tailor-Made Synthesis Of Desired Inorganic Porous Crystalline Materials -- 24.5 Concluding Remarks -- References -- Subject Index.