Microwave-assisted Organic Synthesis : One Hundred Reaction Procedures.
Title:
Microwave-assisted Organic Synthesis : One Hundred Reaction Procedures.
Author:
Bogdal, D.
ISBN:
9780080518732
Personal Author:
Edition:
1st ed.
Physical Description:
1 online resource (215 pages)
Series:
Tetrahedron Organic Chemistry ; v.25
Tetrahedron Organic Chemistry
Contents:
Cover Page -- Title Page -- Copyright Page -- Table of Contents -- Preface -- Acknowledgements -- Chapter 1 Interaction of microwaves with different materials -- Chapter 2 Microwave effect vs. thermal effect -- 2.2 Non-thermal activation during microwave irradiation -- Chapter 3 Microwave equipment -- 3.1 Microwave generators -- 3.4 Microwave reactors -- 3.5 Temperature monitoring -- Chapter 4 Reaction vessels and glassware -- Chapter 5 Techniques for conducting chemical reactions under microwave irradiation -- Chapter 6 Safety precautions on the application of microwaves in laboratory -- 7.1.3 Biphenyl -- 7.1.4 l-Nitro-4-phenylethynyl-benzene -- 7.1.5 3-(4-Nitro-phenyl)-acrylic acid ethyl ester -- 7.1.7 2-Imidazol-1-yl-ethanol -- 7.1.9 Cyclohexanon -- 7.1.11 2-Iodo-4-nitroaniline -- 7.1.12 3-Bromocarbazole -- 7.1.13 3,6-Dichlorocarbazole -- 7.1.17 2,4-Dihydroxybenzaldehyde -- 7.1.18 4-Diethylaminosalicylaldehyde -- 7.1.20 8-Hydraxy-l,l,7,7-tetramethyljulolidine -9-carboxaldehyde -- 7.1.21 7-Diethylamino-2-oxo-2H-chromene-3-carboxylic acid -- 7.1.22 1-Iododecane -- 7.2 Reactions of reagents supported on mineral supports -- 7.2.1 Diphenylbutadiyne -- 7.2.2 2,4,5-Triphenylimidazole -- 7.2.3 1-(4-Nitro-phenyl)-piperidine -- 7.2.4 2-Nitro-1-phenyl-propan-1-ol -- 7.2.5 Phenyl-[1-phenyl-methylidene]amine -- 7.2.9 3-Methyl-2-propyl-1H-indole -- 7.2.10 Azepan-2-one (e-caprolactam) -- 7.2.11 Octyl acetate -- 7.2.12 Octanal -- 7.2.18 l-Phenethylindole-2-carboxylic acid ethyl ester -- 7.2.20 N-Benzylphenylacetamide -- 7.3 Solvent-free phase transfer catalysis (PTC) reactions -- 7.3.1 trans-l,2-Diphenylethylene (trans-stilbene) -- 7.3.2 1-Phenyl-naphthalene -- 7.3.5 Naphtho[2,1-b]furan-2-carboxylic acid ethyl ester -- 7.3.7 Octanoic acid -- 7.3.8 Octan-2-one -- 7.3.11 1-Octyl-azepan-2-one (N-Octylcaprolactam).
7.3.16 N-(2,3-Epoxypropyl)carbazole -- 7.3.20 l,12-Bis(furan-2-ylmethoxy)dodecane -- 7.4 Reactions of neat reagents -- 7.4.1 7,7-Dimethyl-4-phenyl-4,6,7,8-tetrahydro-1H,3H-quinoline-2,5-dione -- 7.4.2 N-Benzyl-phthalimide -- 7.4.3 N-Phthaloylglycine -- 7.4.6 (E)-l,3-Diphenyl-propenone (chaleone) -- 7.4.7 Beta-Nitrostyrene -- 7.4.8 Phenyl-[1-phenyl-methylidene]amine -- 7.4.9 2-Oxo-2H-chromene-3-carboxylic acid ethyl ester -- 7.4.10 7-Diethylamino-2-oxo-2H-chromene-3-carboxylic acid ethyl ester -- 7.4.12 trans-1,2-Diphenylethylene (trans-stilbene) -- 7.4.13 2-Benzylidene-malononitrile -- 7.4.14 Diethyl benzylidenemalonate -- 7.4.16 2-Methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydro-pyridine-3-carboxylic acid ethyl ester -- 7.4.17 2-Oxo-2H-chromene-3-carboxylic acid -- 7.4.18 Bromocyclohexane -- 7.4.19 1-(4-Nitro-phenyl)-piperidine -- 7.4.20 2-Acetoxy-benzoic acid (aspirine) -- 7.4.22 3-[1-Phenyl-methylidene]-3H-isobenzofuran-1-one -- 7.4.25 trans-9,10-Dihydro-9,10-ethanoanthracene dicarboxylic acid dimethyl ester -- 7.5.2 Poly(butyl acrylate) -- 7.5.5 Poly(2-(9-carbazolylethyl methacrylate) -- 7.5.6 Polystyrene -- 7.5.7 High molecular weight (solid) epoxy resins - bisphenol A -- 7.5.8 High molecular weight (solid) epoxy resins - 1,1'-Bi-2-naphthol -- 7.5.11 Polyethers -- 7.5.13 Polyphosphazene -- Index.
Abstract:
Microwave-assisted Organic Synthesis - One Hundred Reaction Procedures provides readers with a broad overview of microwave assisted Organic Synthesis, enabling students and researchers alike to produce more efficient and high yield syntheses while saving time and resources. The work addresses key problems faced by chemistry laboratories in academia and in industry, that of an ever increasing need for procedures which are low-waste, energy efficient, high yield, occur over a short reaction period, and use environmentally friendly solvents. All these factors play an important role in the development of Green Chemistry methods, and in this, Microwave-assisted Organic Synthesis - One Hundred Reaction Procedures is an excellent resource for any library. * Provides a broad overview of microwave enhanced chemistry * Extensive references to the source of each procedure, including equipment used, full operating procedure, and associated hazards * Includes exercises and worked problems which can support more independent study.
Local Note:
Electronic reproduction. Ann Arbor, Michigan : ProQuest Ebook Central, 2017. Available via World Wide Web. Access may be limited to ProQuest Ebook Central affiliated libraries.
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